Article Figures & Data
Tables
Analysis method % RCP at time after reconstitution (mean ± SE) Accuracy of method (%) 30 min 120 min 360 min Baker-Flex SG/EtAc 98.3 ± 0.8 (n = 5) — — 1.8 W17/EtAc 97.8 ± 0.3 (n = 19) 98.8 ± 0.8 (n = 3) 98.7 ± 0.3 (n = 3) 1.3 C18/saline, regular 98.2 ± 0.2 (n = 19) 98.0 ± 0.5 (n = 3) 99.0 ± 0.4 (n = 3) 1.0 C18/saline, fast 93.8 ± 0.4 (n = 19) 93.8 ± 0.5 (n = 3) 94.8 ± 0.4 (n = 3) 1.8 ITLC SG/saline 97.4 ± 0.1 (n = 3) 98.6 ± 0.0 (n = 3) 97.0 ± 0.3 (n = 3) 0.2 SAX/WFI 96.0 ± 1.2 (n = 3) — — 2.1 SG = silica gel; EtAc = ethylacetate; W17 = Whatman 17; SAX = strong anion exchange.
Analysis method P value at time after reconstitution W17/EtAc C18/saline, regular ITLC SG/saline 30 min 120 min 360 min 30 min 120 min 360 min 30 min 120 min 360 min Baker-Flex SG/EtAc 0.56 — — 0.71 — — 0.24 — — W17/EtAc — — — 0.80 0.24 0.37 0.73 0.45 0.03 C18/saline, regular — — — — — — 0.51 0.20 0.01 C18/saline, fast — — — <0.001 <0.001 <0.001 — — — W17 = Whatman 17; EtAc = ethyl acetate; SG = silica gel.